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Beilstein J. Org. Chem. 2020, 16, 185–189, doi:10.3762/bjoc.16.21
Graphical Abstract
Scheme 1: Our strategy.
Scheme 2: Allylic cross-coupling using aldehydes as α-alkoxyalkyl anions.
Scheme 3: Substrate scope and reaction conditions. a) reactions were carried out with 1 (0.4 mmol), 2 (0.2 mm...
Scheme 4: Stoichiometric reaction.
Scheme 5: Possible pathway.
Beilstein J. Org. Chem. 2015, 11, 2444–2450, doi:10.3762/bjoc.11.265
Scheme 1: Conjugate addition of alkylborane 2a to alkynoate 3a.
Scheme 2: Synthesis of five membered carbocycle.
Scheme 3: Deuterium-labeling experiment.
Figure 1: Possible mechanism.
Figure 2: Isomerization of the alkenylcopper intermediates.